Coskun, A.Koc, Z. E.2020-03-262020-03-2620071070-3284https://dx.doi.org/10.1134/S1070328407030050https://hdl.handle.net/20.500.12395/216304-Acetyldiphenyl sulfide and 4.4'-diacetyidiphenyl sulfide were synthesized from diphenyl sulfide and acetyl chloride in the presence of AlCl3 as catalyst in the Friedel-Crafts reaction. Subsequently, the ketooxime and glyoxime derivatives were also prepared. The metal complexes of the glyoximes, such as copper, nickel, and cobalt complexes were prepared. The BF2+ capped Ni(II) mononuclear complex of 4-thiophenoxyphenylglyoxime was prepared. The structures of these ligands were identified by FT-IR, H-1 NMR, and C-13 NMR spectral data and elemental analysis. The structures of the complexes were identified by FT-IR, elemental analysis, and magnetic measurements.en10.1134/S1070328407030050info:eu-repo/semantics/closedAccessArticle333184189Q3WOS:000245356900005Q4