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Öğe Conventional and high intensity halogen light effects on water sorption and microhardness of orthodontic adhesives(E H ANGLE EDUCATION RESEARCH FOUNDATION, INC, 2008) Uysal, Tancan; Basciftci, Faruk Ayhan; Sener, Yagmur; Botsali, Murat Selim; Demir, AbdullahObjective: To test the null hypothesis that when the equivalent total light energy is irradiated to three orthodontic adhesive resins, there is no difference between the microhardness and water sorption values regardless of the curing light sources. Materials and Methods: Samples were divided into six groups according to the combination of three orthodontic adhesives (Kurasper F, Light-Bond, Transbond XT) and two light intensities (quartz tungsten halogen [QTH] and high intensity quartz tungsten halogen [HQTH]). One half of each of the 40 samples of three adhesive pastes was polymerized for 20 seconds by a QTH light source, and the other half was polymerized for 10 seconds by a HQTH light source. Water sorption was determined and Vickers hardness was established with three measurements per sample at the top, center, and bottom. Statistical analysis was performed using two-way analysis of variance (ANOVA) with multiple comparisons (Tukey-HSD). Results: Statistically significant differences were found among all adhesives for water sorption and hardness values cured with QTH and HQTH. The HQTH curing unit resulted in higher values than did the QTH. The highest water sorption values were observed for Kurasper F cured with HQTH and the lowest value was observed for Transbond XT cured with QTH. For microhardness Light-Bond cured with HQTH produced the highest values, and Transbond XT cured with QTH produced the lowest. Conclusions: When the equivalent total light energy is irradiated to three orthodontic adhesive resins, there are significant differences between the microhardness and water sorption values cured with the QTH and HQTH light source. The null hypothesis is rejected.Öğe Effect of alternative modes of application on microleakage of one-step self-etch adhesives(ELSEVIER TAIWAN, 2013) Ulker, Mustafa; Ulker, Hayriye Esra; Karabekiroglu, Said; Botsali, Murat Selim; Cetin, Ali RizaBackground/purpose: Contemporary one-step self-etch adhesives are certainly the most user-friendly adhesives; however, typically could not compete with the more traditional multi-step adhesives. This in vitro study evaluated the efficacy of two modes of application (double application or placement of a hydrophobic resin coating) for the reduction of microleakage, using three different one-step self-etch adhesives (AdheSE One VivaPen, lvoclar Vivadent, Schaan, Liechtenstein; Xeno V, Dentsply De Trey, Konstanz, Germany; OptiBond All-In-One, Kerr Italia S.r.l, Scafati, Italy). Materials and methods: We prepared Class V cavities with the occlusal margin in enamel and gingival margin in dentin on both buccal and lingual surfaces of 108 human molar teeth. Cavities were divided into nine groups according to the combination of adhesives and application modes used (n = 24). For applying adhesives, we followed three types of procedures: (1) according to the manufacturers' directions; (2) using a double-application method; and (3) with the additional placement of a hydrophobic resin layer after following the manufacturers' directions. We restored the cavities with a composite resin. After thermocycling (500 cycles at 5 degrees C/55 degrees C) and immersion in 0.5% basic fuchsin, we sectioned the teeth and evaluated them for microleakage using a stereo microscope (20x). Enamel and dentin margins were scored separately, and we analyzed the data using Kruskal-Wallis, Bonferroni-corrected Mann-Whitney U, and Wilcoxon signed-rank tests. Results: Application of a hydrophobic resin over the cured Xeno V adhesive decreased the amount of microleakage at the enamel margins, compared with the application according to the manufacturer's instructions (P = 0.005). Both application modes decreased the amount of microleakage at the dentin margins with AdheSE One VivaPen adhesive, compared with application according to the manufacturer's instructions (P < 0.001). With the OptiBond All-In-One adhesive, no significant difference between application modes was observed. Conclusion: Alternative modes of application did not adversely affect the sealing ability of one-step self-etch adhesives. Depending on the type of adhesive, alternative modes of application may contribute to low microleakage values. Copyright (C) 2012, Association for Dental Sciences of the Republic of China. Published by Elsevier Taiwan LLC. All rights reserved.Öğe Effect of different surface treatments on the microtensile bond strength of two self-adhesive flowable composites(SPRINGER LONDON LTD, 2015) Altunsoy, Mustafa; Botsali, Murat Selim; Sari, Tugrul; Onat, HalenurThe aim of this study was to evaluate the effect of different surface treatments on the microtensile bond strength (mu TBS) of two different self-adhesive flowable composite materials (SACs) to dentin. Forty extracted human molars were horizontally flattened to expose the dentin surfaces. The teeth were divided into eight groups according to the surface treatments (acid etching, Er:YAG laser quantum square pulse (QSP) mode, and Er:YAG laser medium-short pulse (MSP) mode at 10 Hz, 1.2 W, 120 mJ, and control-SiC) and SAC type (Vertise Flow and Fusio Liquid Dentin) (n = 5). Light cured 4-mm-high composite build-ups were made on the dentin surfaces, and the specimens were sectioned into serial sticks (n = 15). Later, the specimens were attached to microtensile testing machine and tensile force was applied at a crosshead speed of 1 mm/min until failure occurred. The failure modes were evaluated using a stereomicroscope at x40 magnification, and one sample from each group was used for scanning electron microscopy (SEM) evaluation. The data were analyzed with two-way ANOVA and Tukey's HSD test (alpha = 0.05). In all surface treatment groups along with the control groups, Vertise Flow showed better mu TBS than the Fusio Liquid Dentin with the exception of the Er:YAG MSP mode surface treatment (p < 0.05). Etching with phosphoric acid and the Er:YAG QSP mode surface treatment significantly increased the mu TBS of Vertise Flow (p < 0.05). Etching with phosphoric acid, Er:YAG QSP mode surface treatment, and Er:YAG MSP mode surface treatment significantly increased the mu TBS of Fusio Liquid Dentin (p < 0.05). The mu TBS of Vertise Flow was higher than the mu TBS of Fusio Liquid Dentin. The Er:YAG laser irradiation increased the mu TBS of both self-adhesive flowable resin composites in two pulse modes tested (MSP or QSP). However, the highest mu TBS was recorded when Vertise Flow was applied with acid etching.Öğe Effect of different surface treatments on the shear and microtensile bond strength of resin-modified glass ionomer cement to dentin(TAYLOR & FRANCIS LTD, 2014) Altunsoy, Mustafa; Botsali, Murat Selim; Korkut, Emre; Kucukyilmaz, Ebru; Sener, YagmurObjective. The aim of this study was to evaluate the effect of different surface treatments on the microtensile bond strength (mTBS) and shear bond strength (SBS) of resin-modified glass ionomer cement (RMGIC) to dentin. Materials and methods. Fifty-two extracted human molars were flattened to obtain dentin surfaces. For SBS assessment 40 teeth were divided into four groups according to their surface treatments (acid etching, Er: YAG laser QSP mode, Er: YAG laser MSP mode and control-SiC) (n = 10). A plastic cylinder was placed over the differently treated dentin surfaces and RMGIC was placed into the rings and polymerized. Twelve teeth were used for the mu TBS test. The treated dentin surfaces described above were restored with 4 mm high RMGIC and light cured; then, the specimens were sectioned into serial sticks (n = 15) and mu TBS and SBS were tested for failure in a testing machine with a 1 mm/min crosshead speed. The data were analyzed by one-way ANOVA and Tukey HSD tests (alpha = 0.05). Results. Acid etching showed significantly higher SBS than the other groups (p < 0.05). Er: YAG QSP and MSP-treated groups showed higher SBS values than the control group, but the difference was not statistically significant (p > 0.05). Er: YAG MSP showed the highest mu TBS value followed by acid etching, whereas the control group exhibited the lowest value (p < 0.05) and the differences between the control group and Er: YAG QSP were not significant (p > 0.05). Conclusions. The application of Er: YAG MSP mode and acid etching to dentin can be used for improving the bond strength of RMGIC.Öğe Effect of increased exposure times on amount of residual monomer released from single-step self-etch adhesives(SAGE PUBLICATIONS LTD, 2015) Altunsoy, Mustafa; Botsali, Murat Selim; Tosun, Gonca; Yasar, AhmetBackground: The aim of this study was to evaluate the effect of increased exposure times on the amount of residual Bis-GMA, TEGDMA, HEMA and UDMA released from single-step self-etch adhesive systems. Methods: Two adhesive systems were used. The adhesives were applied to bovine dentin surface according to the manufacturer's instructions and were polymerized using an LED curing unit for 10, 20 and 40 seconds (n = 5). After polymerization, the specimens were stored in 75% ethanol-water solution (6 mL). Residual monomers (Bis-GMA, TEGDMA, UDMA and HEMA) that were eluted from the adhesives (after 10 minutes, 1 hour, 1 day, 7 days and 30 days) were analyzed by high-performance liquid chromatography (HPLC). The data were analyzed using 1-way analysis of variance and Tukey HSD tests. Results: Among the time periods, the highest amount of released residual monomers from adhesives was observed in the 10th minute. There were statistically significant differences regarding released Bis-GMA, UDMA, HEMA and TEGDMA between the adhesive systems (p<0.05). There were no significant differences among the 10, 20 and 40 second polymerization times according to their effect on residual monomer release from adhesives (p>0.05). Conclusions: Increasing the polymerization time did not have an effect on residual monomer release from single-step self-etch adhesives.Öğe Effect of new innovative restorative carbomised glass cement on intrapulpal temperature rise: an ex-vivo study(SOCIEDADE BRASILEIRA DE PESQUISA ODONTOLOGICA, 2016) Botsali, Murat Selim; Tokay, Ugur; Ozmen, Bilal; Cortcu, Murat; Koyuturk, Alp Erdin; Kahvecioglu, FirdevsThis study aimed to evaluate the temperature changes that occurred in the pulp chamber when using GCP Glass Carbomer Fill (GCP) and two different resin-modified glass-ionomer (RGI) restorative materials at different dentin thicknesses. A standardized Class I occlusal cavity with 1 mm or 2 mm dentin thickness was prepared in the extracted human molar teeth. RGI and GCP fills were placed in the cavities and cured with two different light-curing units. This study included a total of 120 samples, with 20 samples in each group. The pulp microcirculation method was used for measuring the intrapulpal temperature changes. Statistical analysis was performed using the two-way ANOVA and Tukey HSD multiple comparison tests. Statistically significant differences were observed between 1 mm and 2 mm dentin thicknesses (p < 0.001). The GCP groups (both 1 mm and 2 mm dentin thicknesses) exhibited higher temperatures than the other groups (p < 0.001), and Fuji II LC and Photac Fil Quick Aplicap showed similar values (p > 0.05). The highest temperature changes were observed with 1 mm dentin thickness. While RGI materials in both dentin thicknesses did not cause temperature changes that were harmful to the pulp, GCP CarboLED LCU caused the highest intrapulpal temperature rise, and these values were borderline harmful to the dental pulp.Öğe Evaluation of HEMA released from four different adhesive systems by HPLC(SAGE PUBLICATIONS LTD, 2015) Altunsoy, Mustafa; Botsali, Murat Selim; Ulker, Hayriye EsraPurpose: This study evaluated the elution of 2-hydroxyethyl methacrylate (HEMA) from 4 different adhesives, using high-performance liquid chromatography (HPLC). Materials and methods: The adhesives were applied on a bovine dentin surface and polymerized using an LED curing unit (n=5). After polymerization, specimens were stored in 75% ethanol solution (6 mL). Residual HEMA that was eluted from adhesives (after 10 minutes, 1 hour, 24 hours, 7 days and 30 days) was analyzed using HPLC. Statistical analyses were performed using 1-way ANOVA, Tukey HSD test and paired 2-sample t-test. Results: There were statistically significant differences among adhesive systems for the cumulative released HEMA and among the time periods (p<0.05). Clearfil SE Bond showed the highest amount of HEMA released, while Easy Bond showed the lowest. Among the time periods, the highest eluted HEMA value was detected in 10 minutes for all adhesives, and elution continued for up to 30 days. Conclusions: The HEMA eluted from adhesives was in different amounts, and the elution continued for a long time. The amount of eluted HEMA from adhesives used in this study was not viewed as critical for toxic reactions in biological tissues.Öğe Residual monomer release from orthodontic adhesives cured with different light sources(TAYLOR & FRANCIS LTD, 2016) Botsali, Murat Selim; Sozer, Ozlem Akinci; Altunsoy, Mustafa; Demir, Abdullah; Ulker, Hayriye EsraIntroduction: The aim of this study was to evaluate the residual monomer release from orthodontic adhesives cured with light-emitting diode (LED) and halogen light sources.Methods: Seven hundred and twenty stainless steel brackets were divided into 3 groups according to the adhesive system used (Transbond XT light-cure adhesive [TXT], Transbond LR capsule [LR], and Light Bond light-cure adhesive paste [LB]), and each group was divided into 2 subgroups according to light-curing procedure (LED or halogen). Brackets were bonded with adhesives onto tooth buccal surfaces and polymerized. Each specimen contained 24 brackets that simulated the oral environment (n=5). The specimens were immersed in a 75% ethanol/water solution at 37 degrees C for 10min, 1h, 1 d, 7 d, 14 d, and 30 d, respectively. Eluted monomers (Bis-GMA, UDMA, and TEGDMA) were detected using HPLC.Results: There was residual monomer release at all time periods, and the highest amount of release was observed cumulatively on the 30th day. The cumulative Bis-GMA released from adhesives was not different (p>0.05). The cumulative TEGDMA released from adhesives was statistically different (p<0.05). There was no statistical difference between QTH and LED light-curing units for each adhesive (p>0.05).Conclusions: The release of residual monomers stays at a high level for a long time after polymerization. The total leaching of residual monomers from the Light Bond light-cure sealant resin plus Light Bond light-cure adhesive paste was higher than that of other materials for both curing units. Different curing units (LED or QTH) did not affect the monomer release from the orthodontic adhesives.Öğe Treatment of post-orthodontic white spot lesions with CPP-ACP paste: A three year follow up study(JAPANESE SOC DENTAL MATERIALS DEVICES, 2017) Karabekiroolu, Said; Unlu, Nimet; Kucukyilmaz, Ebru; Sener, Sevgi; Botsali, Murat Selim; Malkoc, SiddikTo determine the efficacy of topical applications of 10% casein phosphopeptide-amorphous calcium phosphate (CPP-ACP) paste in reverting white spot lesions (WSLs) after fixed orthodontic treatment. Forty one participants were randomly assigned to either the test group (CPP-ACP) or the control group (only fluoride toothpaste). All patients used regular fluoride-containing toothpaste. CPP-ACP paste or fluoridated toothpaste was applied on to tooth surfaces with WSLs twice a day during 36-month after de-bonding. The labial/buccal surfaces of teeth were assessed by use of DIAGNOdent pen (DD), Gorelick Index and ICDAS II criteria at baseline (T1) and 36-month (T2) follow-up visits. The total counts of Streptococcus mutans and Lactobacillus were obtained at T1 and T2. DMFT, DMFS, stimulated flow rate and buffer capacity were calculated in two appointments. Daily usage of CPP-ACP paste was not better than normal care for improving the appearance of WSLs after 36 months.
