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Öğe Synthesis of four new vic-dioximes and their nickel(II), cobalt(II), copper(II) and cadmium(II) complexes(KLUWER ACADEMIC PUBL, 2002) Ozcan, E; Karapinar, E; Demirtas, BFour unsymmetrical vic-dioximes: [(LH2)-H-1] N-(4-butylphenyl)amino-amphi-glyoxime, [(LH2)-H-2] N-(4-butylphenyl)amino-anti-glyoxime, [(LH2)-H-3] N-(4-phenylazophenyl)amino-amphi-glyoxime and [(LH2)-H-4] N-(4-phenylazophenyl)amino-anti-glyoxime have been prepared from amphi-chloroglyoxime, anti-chloroglyoxime, 4-butylaniline and 4-(phenylazo)aniline respectively. The complexes of these vic-dioximes with (NiI)-I-I, (CoI)-I-I, (CuI)-I-I and (CdI)-I-I ions have been investigated. All are insoluble in common solvents. Their i.r. spectra and elemental analyses are given, together with mass and H-1-n.m.r. spectra of the ligands.