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Öğe Effect of silica/graphene nanohybrid particles on the mechanical properties of epoxy coatings(SPRINGER HEIDELBERG, 2019) Ozcan, Umit Esra.; Karabork, Fazliye.; Yazman, Sakir.; Akdemir, Ahmet.Epoxy resins are used as coating materials, but the practical use of epoxy coatings in industries is limited due to their weak mechanical properties. In the present paper, different amounts of silica nanoparticles (SiO2) and graphene nanoplatelets (GNPs) were introduced separately and together into an epoxy coating matrix as reinforcements. Graphene, a newly discovered carbon allotrope, has been found to improve the mechanical properties of the polymer composites in which it is dispersed. Silica particles are also known to improve the mechanical properties of composites. In this study, mechanical, physical and thermal properties of the epoxy coatings are considered as multidimensional by the macro- and microanalyses. The experimental results showed that after the addition of GNPs into the epoxy matrix, the flexibility and impact resistance of the coatings increased by 8.3 and 157.1%, respectively, in relation to neat epoxy. The microhardness increased by 53.8% and penetration depth, which is indicative of the scratch resistance, decreased by 29.7%, with the addition of SiO2-GNPs nanohybrid. A remarkable synergistic effect was observed between the GNPs and SiO2, which improved the hardness and the scratch resistance of the epoxy coatings.Öğe Evaluation of flexural strength of different denture base materials reinforced with different nanoparticles(WILEY, 2019) Karci, Muhammet.; Demir, Necla.; Yazman, Sakir.Purpose To evaluate the effect of adding Al2O3, SiO2, and TiO2 nanoparticles in ratios of 1, 3, and 5 wt% to different acrylic resins on flexural strength. Materials and Methods A total of 210 specimens were prepared in 30 groups (n = 7/group) (Control, 1% Al2O3, 3% Al2O3, 5% Al2O3, 1% SiO2, 3% SiO2, 5% SiO2, 1% TiO2, 3% TiO2, 5% TiO2). The specimens were polished with 200-, 400-, and 600-grit abrasive paper to provide a standard surface before testing and then suspended in distilled water for 30 days. Flexural strength was measured via three-point bending tests. Subsequently, SEM analysis was performed for one specimen from each group. Homogeneity of data was assessed by Kolmogov-Smirnov test followed by two-way ANOVA and Tukey HSD tests (alpha = 0.05). Results There was a significant increase in the flexural strength of polymethylmethacrylate (PMMA) after addition of 1% nanoparticles in both heat-polymerized and autopolymerized acrylic resins (p < 0.05). The flexural strength values of the groups to which Al2O3 and TiO2 nanoparticles were added exceeded those of the group with SiO2 addition (p < 0.05). The electron microscopy images revealed that the nanoparticles were more homogeneously dispersed in PMMA with higher flexural strength. Conclusions The mechanical properties of PMMA can be improved by the addition of nanoparticles to PMMA; however, the flexural strength values of PMMA decrease with the addition of nanoparticles at higher percentages (3-5%). Hence, the ideal filler ratio corresponds to 1%.