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Öğe New glyoxime derivatives and their transition metal complexes(PLEIADES PUBLISHING INC, 2007) Yildirim, B.; Oezcan, E.; Deveci, P.Two new vic-dioxime ligands and their complexes with Co+2, Ni+2, Cu+2, Cd+2, and Zn+2 ions were synthesized. Primer amines (3,4-methylenedioxaaniline and 4-methylbenzylamine) reacted with antichloroglyoxime to give 3,4-methylenedioxaphenylaminoglyoxime (H2L1) and N-(4-methylbenzyl)aminoglyoxime (H2L2) ligands. Structures of the ligands and their complexes are proposed based on elemental analyses, IR, UV-Vis, and H-1 NMR spectra, magnetic susceptibility measurements, and thermogravi metric analyses (TGA).