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    Synthesis and complexation of two new phenylaminoglyoxime ligands
    (TAYLOR & FRANCIS LTD, 2008) Deveci, Pervin; Ozcan, Emine; Taner, Bilge; Arslan, Oemer
    Two new soluble phenylaminoglyoxime ligands, 4-isopropylanilinephenylglyoxime ((LH2)-H-1), 4-benzylpiperidinephenylglyoxime ((LH2)-H-2), were prepared by reacting 4-isopropylaniline and 4-benzylpiperidine with chlorophenylglyoxime. Mononuclear nickel(II), cobalt(II), copper(II), zinc(II), and cadmium(II) complexes with these ligands were synthesized. On the basis of the magnetic and spectral evidence a square-planar geometry for Ni(II) and Cu(II) complexes, a tedrahedral geometry for Cd(II) and Zn(II) complexes and octahedral geometry for Co(II) complexes are proposed. These compounds were elucidated by elemental analysis, IR, UV-Vis, and magnetic moments. The ligands were additionally characterized by H-1 NMR and C-13 NMR spectra.