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Öğe The Synthesis and Ni(Ii), Co(Ii) and Cu(Ii) Complexes of Three New Unsymmetrical Vic-Dioximes(MARCEL DEKKER INC, 1995) Deveci, M. All; Irez, Gazi; Mercimek, Bedrettin; Bedük, A. Dinçer; Sarıkavaklı, NursabahThe reaction of anti-chlorophenylglyoxime with suitable alkylamines in ethanol-water at 0 degrees C gives the unsymmetrical vic-dioximes, namely, N-ethylaminophenylglyoxime (L(1)H(2)), N-propylaminoglyoxime (L(2)H(2)) and N-butylaminoglyoxime (L(3)H(2)). The Ni(li) and Cu(II) complexes of these ligands are square-planar while the Co(II) complexes are octahedral with water molecules as axial ligands. The structures of these complexes are proposed based on elemental analyses, IR and magnetic susceptibility measurements.