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    The Synthesis of Four New Schiff Bases and Some of Their Transition Metal Complexes
    (MARCEL DEKKER INC, 1998) Uçan, H. I.; Karataş, I.; Irez, G.; Deveci, M. A.; Mercimek, B.
    Isonitrosoacetophenone, synthesized by nitrosotion of acetophenone, has been condensed with diamines (1,4-phenylenediamine, 4,4'-diaminobiphenyl, 4,4'-diaminodiphenylmethane or 4,4'-diaminodiphenylether) to obtain the tetradentate Schiff bases 1,4-phenyliminobis(isonitrosoacetophenone), 1,1'-biphenyl-4,4'-diiminobis(isonitrosoacetophenone), 1,1'-diphenylmethane-4,4'-diiminobis(isonitrosoacetophenone) or 1,1'-diphenyloxy-4,4'-diiminobis(isonitrosoacetophenone). The polymeric Ni(II) and Cu(II) complexes of these Schiff bases are square-planar while the polymeric Co(II) complexes are octahedral with water molecules at the axial positions. The structures of the above complexes were determined by H-1 NMR and IR spectroscopy and elemental analyses.
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    Synthesis of Some Polyamidoximes and Their Complexes With Ni(ii), Co(ii), and Cu(ii) Salts
    (MARCEL DEKKER INC, 1993) Karataş, I.; Irez, G.
    In this study synthesis of four polyamidoximes from their corresponding aromatic diamines and anti-dichloroglyoxime were presented. Average molecular weight of the polymers were determined. In addition, the complex preparation of the above polymeric ligands, with Ni(II), Co(II) and Cu(II) salts were described. Elemental analyses, along with the IR and H-1-NMR spectral techniques were employed, in order to elucidate the structure of the polymeric ligands. and their complexes.