L-lysine derived nickel nanoparticles for reductive degradation of organic dyes

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dc.contributor.authorKhaskheli, Abdul Rauf
dc.contributor.authorNaz, Saba
dc.contributor.authorSoomro, Razium Ali
dc.contributor.authorÖzül, Faruk
dc.contributor.authorAljabour, Abdalaziz
dc.contributor.authorKalwar, Nazar Hussain
dc.contributor.authorMahesar, Abdul Waheed
dc.contributor.authorPatır, Hatay İmren
dc.contributor.authorErsöz, Mustafa
dc.date.accessioned2020-03-26T19:32:01Z
dc.date.available2020-03-26T19:32:01Z
dc.date.issued2016
dc.departmentSelçuk Üniversitesien_US
dc.description.abstractThis report demonstrates a facile and green fabrication method for the nickel nanoparticles using L-lysine as an efficient protecting agent. The application of green amino acid (L-lysine) enabled formation highly spherical and well-dispersed nanoparticles with average diameter in the range of 10 ±2.5 nm. UV-Vis spectroscopy was used as a primary tool to elaborately study and optimize the necessary experimental condition for the developed synthetic protocol. Fourier transform infrared spectroscopy (FTIR) was used to confirm the surface protection of Ni NPs via L-lysine molecules whereas; atomic force microscopy (AFM) and scanning electron microscopy (SEM) provided morphological and topographical view of the as-synthesized Ni NPs. In addition, small angle X-ray scattering (SAXS) and X-ray diffraction (XRD) were used to evaluate compositional characteristics of fabricated L-lysine protected Ni NPs. The as-synthesized Ni NPs demonstrated excellent catalytic potential when utilized as heterogeneous catalyst for reduction of methylene Blue (MB) in the presence of sodium borohydride (NaBH4). The observed catalytic reaction was determined to follow pseudo first order kinetics with rate constant (K) and turn over frequency (TOF) determined to be 0.0224 and TOF value of 0.00411 s-1 respectively. © 2016 VBRI Press.en_US
dc.identifier.doi10.5185/amlett.2016.6215en_US
dc.identifier.endpage621en_US
dc.identifier.issn0976-3961en_US
dc.identifier.issue8en_US
dc.identifier.scopusqualityN/Aen_US
dc.identifier.startpage616en_US
dc.identifier.urihttps://dx.doi.org/10.5185/amlett.2016.6215
dc.identifier.urihttps://hdl.handle.net/20.500.12395/34289
dc.identifier.volume7en_US
dc.indekslendigikaynakScopusen_US
dc.language.isoenen_US
dc.publisherVBRI Pressen_US
dc.relation.ispartofAdvanced Materials Lettersen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.selcuk20240510_oaigen_US
dc.subjectAFMen_US
dc.subjectL-lysineen_US
dc.subjectMethylene blueen_US
dc.subjectMFMen_US
dc.subjectNickel nanoparticlesen_US
dc.subjectSEMen_US
dc.subjectXRDen_US
dc.titleL-lysine derived nickel nanoparticles for reductive degradation of organic dyesen_US
dc.typeArticleen_US

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