Synthesis and characterization of 4-arylaminobiphenylglyoximes and their complexes

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dc.contributor.authorKaripcin, Fatma
dc.contributor.authorArabali, Filiz
dc.contributor.authorKaratas, I.
dc.date.accessioned2020-03-26T17:04:24Z
dc.date.available2020-03-26T17:04:24Z
dc.date.issued2006
dc.departmentSelçuk Üniversitesien_US
dc.description.abstract4-Chloroacetylbiphenyl has been synthesized by Friedel-Crafts reaction between biphenyl and chloroacetyl chloride in the presence of AlCl3 catalyst. The nitrosation reaction of this compound gave 4-biphenylhydroxamyl chloride (HL). Subsequently, 4-biphenylchloroglyoxime (H2L) was prepared by the reaction of 4-biphenylhydroxamyl chloride and hydroxylamine hydrochloride. Then, six new substituted 4-biphenylaminoglyoximes (H2Lx) have been synthesized from 4-biphenylchloroglyoxime and the corresponding amines. A series of M(II)-dioxime complexes of the type [M(HLx)(2)] or [M(HLx)(2) (H2O)(2)] [M(II)=Co(II), Ni(II), Cu(II)] have been synthesized and characterized by FT-IR, H-1 NMR spectral studies, elemental analysis, AAS and magnetic susceptibility measurements.en_US
dc.identifier.endpage985en_US
dc.identifier.issn0717-9324en_US
dc.identifier.issue3en_US
dc.identifier.startpage982en_US
dc.identifier.urihttps://hdl.handle.net/20.500.12395/20695
dc.identifier.volume51en_US
dc.identifier.wosWOS:000240570800012en_US
dc.identifier.wosqualityQ3en_US
dc.indekslendigikaynakWeb of Scienceen_US
dc.language.isoenen_US
dc.publisherSOC CHILENA QUIMICAen_US
dc.relation.ispartofJOURNAL OF THE CHILEAN CHEMICAL SOCIETYen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/openAccessen_US
dc.selcuk20240510_oaigen_US
dc.subjectdioximesen_US
dc.subjectmagnetic propertiesen_US
dc.subjectmetal complexesen_US
dc.subjectFT-IRen_US
dc.titleSynthesis and characterization of 4-arylaminobiphenylglyoximes and their complexesen_US
dc.typeArticleen_US

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