Chemical synthesis of single-layer graphene by using ball milling compared with NaBH4 and hydroquinone reductants

Basit Öğe Kaydı
dc.contributor.authorNiftaliyeva, Aysel
dc.contributor.authorPehlivan, Erol
dc.contributor.authorPolat, Safa
dc.contributor.authorAvci, Ahmet
dc.date.accessioned2020-03-26T19:53:05Z
dc.date.available2020-03-26T19:53:05Z
dc.date.issued2018
dc.departmentSelçuk Üniversitesien_US
dc.description.abstractGraphene materials especially single-layer graphene have been identified as a new generation of nanomaterials having various potential applications in material industries. However, the synthesis procedure of single-layer graphene to improve its quality, size and amount has been still under research for commercial applications. The graphene oxide (GO) is synthesised from graphite by Hummer's spontaneous approach which is the most suitable reaction for a large-scale production. For the single-layer graphene, in this work, GO was exfoliated by using a ball milling in an inert atmosphere. Owing to using ball milling as intermediate treatment degreased oxygen functional groups and number of layers, it facilitates to synthesise graphene. Sodium borohydride (NaBH4) and hydroquinone were used as a reductant for the chemical conversion of the exfoliated GO to graphene. The results showed that due to the strong reduction feature, both reducing agents can be applied in the graphene production. As a preferred reductant, hydroquinone can be successfully applied for the synthesis of the single-layer graphene compared to NaBH4. The obtained graphene particles by two different chemicals were characterised by various analytical techniques. The big difference in the structure of GO and graphene was observed in transmission electron microscope analysis.en_US
dc.description.sponsorshipScientific and Technological Research Council of Turkey (TUBITAK)Turkiye Bilimsel ve Teknolojik Arastirma Kurumu (TUBITAK) [215M777]en_US
dc.description.sponsorshipWe are very appreciative of The Scientific and Technological Research Council of Turkey (TUBITAK) for their support of this investigation (grant no. 215M777).en_US
dc.identifier.doi10.1049/mnl.2018.5165en_US
dc.identifier.endpage1416en_US
dc.identifier.issn1750-0443en_US
dc.identifier.issue10en_US
dc.identifier.scopusqualityQ3en_US
dc.identifier.startpage1412en_US
dc.identifier.urihttps://dx.doi.org/10.1049/mnl.2018.5165
dc.identifier.urihttps://hdl.handle.net/20.500.12395/36396
dc.identifier.volume13en_US
dc.identifier.wosWOS:000451920200011en_US
dc.identifier.wosqualityQ4en_US
dc.indekslendigikaynakWeb of Scienceen_US
dc.indekslendigikaynakScopusen_US
dc.language.isoenen_US
dc.publisherINST ENGINEERING TECHNOLOGY-IETen_US
dc.relation.ispartofMICRO & NANO LETTERSen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.selcuk20240510_oaigen_US
dc.subjecttransmission electron microscopyen_US
dc.subjectreduction (chemical)en_US
dc.subjectgrapheneen_US
dc.subjectball millingen_US
dc.subjectnanofabricationen_US
dc.subjectsingle-layer grapheneen_US
dc.subjectball millingen_US
dc.subjectgraphene oxideen_US
dc.subjectnanomaterialsen_US
dc.subjectHummers spontaneous approachen_US
dc.subjectoxygen functional groupsen_US
dc.subjecttransmission electron microscopyen_US
dc.subjectexfoliationen_US
dc.subjectinert atmosphereen_US
dc.subjectsodium borohydride reductanten_US
dc.subjecthydroquinone reductanten_US
dc.subjectNaBH4en_US
dc.subjectCen_US
dc.titleChemical synthesis of single-layer graphene by using ball milling compared with NaBH4 and hydroquinone reductantsen_US
dc.typeArticleen_US

Dosyalar

Koleksiyon

WoS İndeksli Yayınlar Koleksiyonu
Scopus İndeksli Yayınlar Koleksiyonu