Synthesis and characterization of boron-doped Bi2O3-La2O3 fiber derived nanocomposite precursor

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dc.contributor.authorDurmusoglu, Senol
dc.contributor.authorUslu, Ibrahim
dc.contributor.authorTunc, Tuncay
dc.contributor.authorKeskin, Selda
dc.contributor.authorAytimur, Arda
dc.contributor.authorAkdemir, Ahmet
dc.date.accessioned2020-03-26T18:16:23Z
dc.date.available2020-03-26T18:16:23Z
dc.date.issued2011
dc.departmentSelçuk Üniversitesien_US
dc.description.abstractBoron doped poly(vinyl) alcohol/ bismuth - lanthanum acetate (PVA/Bi-La) nanofibers were prepared by electrospinning using PVA as a precursor. The effect of boron doping was investigated in terms of solution properties, morphological changes and thermal characteristics. The fibers were characterized by FT-IR, XRD, SEM and BET. The addition of boron did not only increase the thermal stability of the fibers, but also their diameters, which yielded stronger fibers. XRD analyses showed that boron doping increased the peak intensities and indicated that the boron doping enhanced the crystallite size. Moreover, no shifts were noticed in diffraction angles for boron doped and undoped samples. Therefore, boron doping did not significantly alter the lattice spacing. The SEM micrograph of the fibers showed that the addition of boron resulted in the formation of cross linked bright surfaced fibers. Also, grain diameters of boron doped and undoped nanocrystalline sintered powders were measured as 170 nm and 120 nm respectively. The BET results show that boron undoped and doped Bi2O3-La2O3 nanocrystalline powder ceramic structures sintered at 800 A degrees C have surface areas of 20.44 m(2)/g and 12.93 m(2)/g, respectively.en_US
dc.description.sponsorshipScientific Research Coordination Center of Selcuk University (BAP)Selcuk Universityen_US
dc.description.sponsorshipFinancial support received from the Scientific Research Coordination Center of Selcuk University (BAP) to conduct the study is gratefully acknowledged.en_US
dc.identifier.doi10.1007/s10965-011-9607-5en_US
dc.identifier.endpage2004en_US
dc.identifier.issn1022-9760en_US
dc.identifier.issn1572-8935en_US
dc.identifier.issue6en_US
dc.identifier.scopusqualityQ2en_US
dc.identifier.startpage1999en_US
dc.identifier.urihttps://dx.doi.org/10.1007/s10965-011-9607-5
dc.identifier.urihttps://hdl.handle.net/20.500.12395/26861
dc.identifier.volume18en_US
dc.identifier.wosWOS:000297352000079en_US
dc.identifier.wosqualityQ2en_US
dc.indekslendigikaynakWeb of Scienceen_US
dc.indekslendigikaynakScopusen_US
dc.language.isoenen_US
dc.publisherSPRINGERen_US
dc.relation.ispartofJOURNAL OF POLYMER RESEARCHen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.selcuk20240510_oaigen_US
dc.subjectElectrospinningen_US
dc.subjectBoric aciden_US
dc.subjectNanofibersen_US
dc.subjectBi-La acetateen_US
dc.subjectPVAen_US
dc.titleSynthesis and characterization of boron-doped Bi2O3-La2O3 fiber derived nanocomposite precursoren_US
dc.typeArticleen_US

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