Determination of Polycyclic Aromatic Hydrocarbons in Soil by Miniaturized Ultrasonic Extraction and Gas Chromatography-Mass Selective Detection

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dc.contributor.authorOzcan, Senar
dc.contributor.authorTor, Ali
dc.contributor.authorAydin, Mehmet Emin
dc.date.accessioned2020-03-26T17:38:13Z
dc.date.available2020-03-26T17:38:13Z
dc.date.issued2009
dc.departmentSelçuk Üniversitesien_US
dc.description.abstractA miniaturized ultrasonic extraction procedure was developed for the determination of polycyclic aromatic hydrocarbons (PAHs) in soil by gas chromatography-mass spectrometry. After determination of the most suitable extraction solvent with 5 min sonication time, several other parameters (sample amount, solvent volume and number of extraction times) were optimized using a 2(3) factorial experimental design. Recoveries of PAHs from spiked soil samples were over 90% for three different fortification levels between 50 and 300 mu g/kg, and relative standard deviations of the recoveries were in the range of < 1 - 15%. The limits of detection ranged from 0.002 to 1.87 mu g/kg. The performance of the developed procedure was also compared with other traditional Soxhlet, shake flask and large scale ultrasonic extraction procedures on real soil samples, and extraction methods showed comparable efficiencies. The proposed procedure required small volumes of solvent and sample. It was practicable, rapid and easy to use for analysis of PAHs in soils.en_US
dc.identifier.doi10.1002/clen.200900110en_US
dc.identifier.endpage817en_US
dc.identifier.issn1863-0650en_US
dc.identifier.issue10en_US
dc.identifier.scopusqualityQ3en_US
dc.identifier.startpage811en_US
dc.identifier.urihttps://dx.doi.org/10.1002/clen.200900110
dc.identifier.urihttps://hdl.handle.net/20.500.12395/23409
dc.identifier.volume37en_US
dc.identifier.wosWOS:000271610300010en_US
dc.identifier.wosqualityQ2en_US
dc.indekslendigikaynakWeb of Scienceen_US
dc.indekslendigikaynakScopusen_US
dc.language.isoenen_US
dc.publisherWILEY-V C H VERLAG GMBHen_US
dc.relation.ispartofCLEAN-SOIL AIR WATERen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.selcuk20240510_oaigen_US
dc.subjectFactorial designen_US
dc.subjectMiniaturized extractionen_US
dc.subjectPolycyclic aromatic hydrocarbonsen_US
dc.subjectSoilen_US
dc.subjectUltrasonic extractionen_US
dc.titleDetermination of Polycyclic Aromatic Hydrocarbons in Soil by Miniaturized Ultrasonic Extraction and Gas Chromatography-Mass Selective Detectionen_US
dc.typeArticleen_US

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