Synthesis and study of the oligo(ether-ester)s based on butylene oxide

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dc.contributor.authorAhmetli, Gulnare
dc.contributor.authorKocak, Ahmet
dc.contributor.authorSoydal, Ulku
dc.date.accessioned2020-03-26T17:27:54Z
dc.date.available2020-03-26T17:27:54Z
dc.date.issued2008
dc.departmentSelçuk Üniversitesien_US
dc.description.abstractUnsaturated oligo(ether-ester) was prepared by ring-opening polymerization of butylene oxide (BO) with glycidyl methacrylate (GMA) in the presence of cationic catalyst (BF3O)-O-center dot(C2H5)(2). The effects of mol ratio of the initial components, amount of catalyst, temperature, and reaction times on the copolymerization reaction were examined. Oligo(ether-ester) were achieved in highest yield of 82% after reaction times of 4 h at 0 degrees C. Synthesized copolymer was characterized using spectroscopic (H-1 NMR and IR) and chemical analysis methods. The thermal degradation and softing points of oligo(ether-ester)-styrene composites were studied. It is shown that crosslinking of the unsaturated oligo(ether-ester) with styrene takes place through the use of thermostable materials. (C) 2008 Wiley Periodicals, Inc.en_US
dc.description.sponsorshipSelcuk University Scientific Research FoundationSelcuk University [2005/05401034]en_US
dc.description.sponsorshipContract grant sponsor: Selcuk University Scientific Research Foundation; contract grant number: 2005/05401034.en_US
dc.identifier.doi10.1002/app.28631en_US
dc.identifier.endpage2020en_US
dc.identifier.issn0021-8995en_US
dc.identifier.issue4en_US
dc.identifier.scopusqualityQ2en_US
dc.identifier.startpage2016en_US
dc.identifier.urihttps://dx.doi.org/10.1002/app.28631
dc.identifier.urihttps://hdl.handle.net/20.500.12395/22670
dc.identifier.volume110en_US
dc.identifier.wosWOS:000259755300016en_US
dc.identifier.wosqualityQ2en_US
dc.indekslendigikaynakWeb of Scienceen_US
dc.indekslendigikaynakScopusen_US
dc.language.isoenen_US
dc.publisherJOHN WILEY & SONS INCen_US
dc.relation.ispartofJOURNAL OF APPLIED POLYMER SCIENCEen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.selcuk20240510_oaigen_US
dc.subjectring-opening polymerizationen_US
dc.subjectcompositesen_US
dc.subjectthermal propertiesen_US
dc.titleSynthesis and study of the oligo(ether-ester)s based on butylene oxideen_US
dc.typeArticleen_US

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