Design and optimization of production parameters for boric acid crystals with the crystallization process in an MSMPR crystallizer using FBRM (R) and PVM (R) technologies

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dc.contributor.authorKutluay, Sinan
dc.contributor.authorSahin, Omer
dc.contributor.authorCeyhan, A. Abdullah
dc.contributor.authorIzgi, M. Sait
dc.date.accessioned2020-03-26T19:34:45Z
dc.date.available2020-03-26T19:34:45Z
dc.date.issued2017
dc.departmentSelçuk Üniversitesien_US
dc.description.abstractIn crystallization studies, newly developed technologies, such as Focused Beam Reflectance Measurement (FBRM) and Particle Vision and Measurement (PVM) are applied for determining on-line monitoring of a representation of the Chord Length Distribution (CLD) and observe the photographs of crystals respectively; moreover recently they are widely used. Properly installed, the FBRM ensures on-line determination of the CLD, which is statistically associated to the Crystal Size Distribution (CSD). In industrial crystallization, CSD and mean crystal size as well as external habit and internal structure are important characteristics for further use of the crystals. In this paper, the effect of residence time, stirring speed, feeding rate, supersaturation level and the polyelectrolytes such as anionic polyacrylamide (APAM) and non-ionic polyacrylamide (NPAM) on the CLD as well as the shape of boric acid crystals were investigated by using the FBRM G600 and the PVM V819 probes respectively in an MSMPR (Mixed Suspension Mixed Product Removal) crystallizer. The CSD and kinetic data were determined experimentally using continuous MSMPR crystallizer running at steady state. The population density of nuclei, the nucleation rate and the growth rate were determined from the experimental population balance distribution when the steady state was reached. (C) 2017 Published by Elsevier B.V.en_US
dc.description.sponsorshipEti Mine Works General Management [ETI MADEN] [17/02/2014-17/01/2016]en_US
dc.description.sponsorshipThis work was supported by Eti Mine Works General Management [ETI MADEN, project number: 17/02/2014-17/01/2016].en_US
dc.identifier.doi10.1016/j.jcrysgro.2017.03.027en_US
dc.identifier.endpage180en_US
dc.identifier.issn0022-0248en_US
dc.identifier.issn1873-5002en_US
dc.identifier.scopusqualityQ2en_US
dc.identifier.startpage172en_US
dc.identifier.urihttps://dx.doi.org/10.1016/j.jcrysgro.2017.03.027
dc.identifier.urihttps://hdl.handle.net/20.500.12395/34949
dc.identifier.volume467en_US
dc.identifier.wosWOS:000401128400027en_US
dc.identifier.wosqualityQ3en_US
dc.indekslendigikaynakWeb of Scienceen_US
dc.indekslendigikaynakScopusen_US
dc.language.isoenen_US
dc.publisherELSEVIER SCIENCE BVen_US
dc.relation.ispartofJOURNAL OF CRYSTAL GROWTHen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.selcuk20240510_oaigen_US
dc.subjectFBRMen_US
dc.subjectPVMen_US
dc.subjectMSMPRen_US
dc.subjectCLDen_US
dc.subjectCrystallizationen_US
dc.subjectBoric aciden_US
dc.titleDesign and optimization of production parameters for boric acid crystals with the crystallization process in an MSMPR crystallizer using FBRM (R) and PVM (R) technologiesen_US
dc.typeArticleen_US

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