Synthesis and characterization of some vic-dioxime and its mononuclear complexes

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dc.contributor.authorUysal, S.
dc.contributor.authorCoskun, A.
dc.contributor.authorKoc, Z. E.
dc.contributor.authorUcan, M.
dc.contributor.authorUcan, H. I.
dc.date.accessioned2020-03-26T17:18:18Z
dc.date.available2020-03-26T17:18:18Z
dc.date.issued2007
dc.departmentSelçuk Üniversitesien_US
dc.description.abstractIn this study, acetophenone is used as a basis substance. omega-Isonitrosoacetophenone has been synthesized from nitrosyl with amyl nitrite of acetophenone in the presence of sodium ethoxide. Subsequently, anti-phenylglyoxime has been prepared by reacting omega-isonitrosoacetophenone with hydroxylamine and sodium acetate in a ethanolic media. Chlorophenylglyoxime has been obtained from reaction with chlorine gases. Then, three aminophenylglyoxime (ligands) have been prepared by the reaction of chlorophenylglyoxime and the corresponding amines. The Ni(II), Co(II), and Cu(II) complexes with BF2+-bridge of anilinophenylglyoxime and 2,4-dimethylanilinophenylglyoxime were prepared. Then polymeric metal complexes with BF2+-bridge of dopamiophenylglyoxime were prepared. Their structures were identified by FT-IR, H-1 NMR, and ICP-AES spectral data, elemental analysis and magnetic measurements.en_US
dc.identifier.doi10.1134/S1070328407050077en_US
dc.identifier.endpage357en_US
dc.identifier.issn1070-3284en_US
dc.identifier.issue5en_US
dc.identifier.scopusqualityQ3en_US
dc.identifier.startpage351en_US
dc.identifier.urihttps://dx.doi.org/10.1134/S1070328407050077
dc.identifier.urihttps://hdl.handle.net/20.500.12395/21632
dc.identifier.volume33en_US
dc.identifier.wosWOS:000247004300007en_US
dc.identifier.wosqualityQ4en_US
dc.indekslendigikaynakWeb of Scienceen_US
dc.indekslendigikaynakScopusen_US
dc.language.isoenen_US
dc.publisherMAIK NAUKA/INTERPERIODICA/SPRINGERen_US
dc.relation.ispartofRUSSIAN JOURNAL OF COORDINATION CHEMISTRYen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.selcuk20240510_oaigen_US
dc.titleSynthesis and characterization of some vic-dioxime and its mononuclear complexesen_US
dc.typeArticleen_US

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