Optimization of the Wet Mechanochemical Process Conditions of SrSO4 to SrCO3 and (NH4)(2)SO4 by Using Response Surface Methodology

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dc.contributor.authorBingöl, Deniz
dc.contributor.authorAydoğan, Salih
dc.contributor.authorKarayünlü Bozbaş, Seda
dc.date.accessioned2020-03-26T18:30:58Z
dc.date.available2020-03-26T18:30:58Z
dc.date.issued2012
dc.departmentSelçuk Üniversitesien_US
dc.description.abstractThe wet mechanochemical process was optimized for insoluble SrCO3 and soluble (NH4)(2)SO4 formation from celestite (SrSO4)-(NH4)(2)CO3-H2O mixtures in a planetary ball mill by Box-Behnken design (BBD). The products formed during wet milling were analyzed with scanning electron microscopy (SEM), X-ray diffraction (XRD), and Fourier transform infrared (FT-IR) spectroscopy. For converting to SrCO3 of celestite (SrSO4) and to (NH4)(2)SO4 of (NH4)(2)CO3, a hydrometallurgical process optimization via the wet mechanochemical conversion using (NH4)(2)CO3 was developed the first time in this work using response surface methodology. The wet mechanochemical conversion was carried out by varying ball to grinding material mass ratio, (NH4)(2)CO3 to SrSO4 mole ratio and the rotational speed of mill in a planetary mill. Under the optimum experimental conditions (9.24 of ball to grinding material mass ratio, 1.86 of (NH4)(2)CO3 to SrSO4 mole ratio and 400 rpm of the rotational speed of mill), the conversion of SrCO3 was 99.08 pct. The (NH4)(2)SO4 obtained as byproduct was crystallized.en_US
dc.description.sponsorshipScientific Research Projects Administration Unit of Kocaeli UniversityKocaeli University [2009/033]en_US
dc.description.sponsorshipThe authors gratefully acknowledge the Scientific Research Projects Administration Unit of Kocaeli University (No. 2009/033) for the economical support granted to the realization of this work.en_US
dc.identifier.citationBingöl, D., Aydoğan, S., Karayünlü Bozbaş, S. (2012). Optimization of the Wet Mechanochemical Process Conditions of SrSO4 to SrCO3 and (NH4)(2)SO4 by Using Response Surface Methodology. Metallurgical and Materials Transactions B-Process Metallurgy and Materials Processing Science, 43(5), 1214-1219. DOI: 10.1007/s11663-012-9687-6
dc.identifier.doi10.1007/s11663-012-9687-6en_US
dc.identifier.endpage1219en_US
dc.identifier.issn1073-5615en_US
dc.identifier.issue5en_US
dc.identifier.scopusqualityQ1en_US
dc.identifier.startpage1214en_US
dc.identifier.urihttps://dx.doi.org/10.1007/s11663-012-9687-6
dc.identifier.urihttps://hdl.handle.net/20.500.12395/28275
dc.identifier.volume43en_US
dc.identifier.wosWOS:000308822100022en_US
dc.identifier.wosqualityQ1en_US
dc.indekslendigikaynakWeb of Scienceen_US
dc.indekslendigikaynakScopusen_US
dc.institutionauthorAydoğan, Salih
dc.language.isoenen_US
dc.publisherSPRINGERen_US
dc.relation.ispartofMetallurgical and Materials Transactions B-Process Metallurgy and Materials Processing Scienceen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/openAccessen_US
dc.selcuk20240510_oaigen_US
dc.titleOptimization of the Wet Mechanochemical Process Conditions of SrSO4 to SrCO3 and (NH4)(2)SO4 by Using Response Surface Methodologyen_US
dc.typeArticleen_US

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