Biogenic silver nanoparticles for trace colorimetric sensing of enzyme disrupter fungicide vinclozolin

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dc.authorid0000-0003-1484-6894
dc.contributor.authorHussain, Masood.
dc.contributor.authorNafady, Ayman.
dc.contributor.authorSirajuddin.
dc.contributor.authorAvcı, Ahmet.
dc.contributor.authorPehlivan, Erol.
dc.contributor.authorNisar, Jan.
dc.contributor.authorSherazi, Syed Tufail Hussain.
dc.contributor.authorBalouch, Aamna.
dc.contributor.authorShah, Muhammad Raza.
dc.contributor.authorAlmaghrabi, Omar A.
dc.contributor.authorUl-Haq, Muhammad Anwar.
dc.date.accessioned2020-03-26T20:12:45Z
dc.date.available2020-03-26T20:12:45Z
dc.date.issued2019
dc.departmentSelçuk Üniversitesi, Mühendislik Fakültesi, Kimya Mühendisliği Bölümüen_US
dc.description.abstractWe report a novel, simple, efficient, and green protocol for biogenic synthesis of silver nanoparticles (AgNPs) in aqueous solution using clove (Syzygium aromaticum) extract as a reducing and protecting agent. Ultraviolet-visible (UV-Vis) spectroscopy was employed to monitor the localized surface plasmon resonance (LSPR) band of clove extract-derived AgNPs prepared under various conditions. Fourier-transform infrared (FTIR) spectroscopy analysis provided information about the surface interaction of the clove extract with the AgNPs. Ultrahigh-resolution transmission electron microscopy (UHRTEM) results confirmed the formation of spherical, uniformly distributed clove extract-capped AgNPs with sizes in the range of 2-20 nm (average size: 14.4 +/- 2 nm). Powder X-ray diffractometry analysis (PXRD) illustrated the formation of pure crystalline AgNPs. These AgNPs were tested as a colorimetric sensor to detect trace amounts of vinclozolin (VIN) by UV-Vis spectroscopy for the first time. The AgNP-based sensor demonstrated very sensitive and selective colorimetric detection of VIN, in the range of 2-16 mu M (R-2 = 0.997). The developed sensor was green, simple, sensitive, selective, economical, and novel, and could detect trace amounts of VIN with limit of detection (LOD) = 21 nM. Importantly, the sensor was successfully employed for the determination of VIN in real water samples collected from various areas in Turkey.en_US
dc.description.sponsorshipTUBITAKTurkiye Bilimsel ve Teknolojik Arastirma Kurumu (TUBITAK) [21514107-115.02-188888]; King Saud University, Riyadh, Saudi ArabiaDeanship of Scientific Research at King Saud University [RSP-2019/79]en_US
dc.description.sponsorshipWe are thankful to TUBITAK for Fellowship provision to the first author via BIDEB 2216 Research Fellowship Program, Ref: 21514107-115.02-188888. This work was also funded through Researchers Supporting Project number (RSP-2019/79) at King Saud University, Riyadh, Saudi Arabia.en_US
dc.identifier.citationHussain, M., Nafady, A., Avcı, A., Pehlivan, E., Nisar, J., Sherazi, S. T. H., Balouch, A., Shah, M. R., Almaghrabi, O. A., Ul-Haq, M. A. (2019). Biogenic Silver Nanoparticles for Trace Colorimetric Sensing of Enzyme Disrupter Fungicide Vinclozolin. Nanomaterials, 9(11), 1604.
dc.identifier.doi10.3390/nano9111604en_US
dc.identifier.issn2079-4991en_US
dc.identifier.issue11en_US
dc.identifier.pmid31726731en_US
dc.identifier.scopusqualityQ1en_US
dc.identifier.urihttps://dx.doi.org/10.3390/nano9111604
dc.identifier.urihttps://hdl.handle.net/20.500.12395/37537
dc.identifier.volume9en_US
dc.identifier.wosWOS:000502271700099en_US
dc.identifier.wosqualityQ2en_US
dc.indekslendigikaynakWeb of Scienceen_US
dc.indekslendigikaynakScopusen_US
dc.indekslendigikaynakPubMeden_US
dc.institutionauthorPehlivan, Erol.
dc.language.isoenen_US
dc.publisherMDPIen_US
dc.relation.ispartofNANOMATERIALSen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/openAccessen_US
dc.selcuk20240510_oaigen_US
dc.subjectclove extracten_US
dc.subjectsilver nanoparticlesen_US
dc.subjectcolorimetric sensoren_US
dc.subjectvinclozolinen_US
dc.subjectreal water samplesen_US
dc.titleBiogenic silver nanoparticles for trace colorimetric sensing of enzyme disrupter fungicide vinclozolinen_US
dc.typeArticleen_US

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