Synthesis and Characterization of Boron Doped Alumina Stabilized Zirconia Fibers

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dc.contributor.authorUslu, I.
dc.contributor.authorTunc, T.
dc.contributor.authorKeskin, S.
dc.contributor.authorOzturk, M. K.
dc.date.accessioned2020-03-26T18:16:23Z
dc.date.available2020-03-26T18:16:23Z
dc.date.issued2011
dc.departmentSelçuk Üniversitesien_US
dc.description.abstractBoron doped PVA/Zr-Al acetate nanofibers were prepared by electrospinning using PVA as a precursor. The effect of calcination temperature on morphology and crystal structure was investigated at 250, 500, and 800 degrees C. The study also establishes the effect of boron doping on the morphology of PVA/Zr-Al acetate nanofibers at various calcination temperatures. The measurements showed that the conductivity, pH, viscosity and the surface tension of the hybrid polymer solutions have increased with boron doping. In addition, the fibers were characterized by FTIR, DSC, XPS, XRD and SEM techniques. The addition of boron did not only increase the thermal stability of the fibers, hut also increased the average fiber diameters, which gave stronger fibers. The DSC results indicated that the melting temperature (Tm) of the fibers was increased from 256 to 270 degrees C with the addition of boron. XRD peak patterns showed that after further heat treatment at 800 degrees C, zirconia exists in two phases of tetragonal and monoclinic modifications. Moreover, alumina does not transform into the gamma-Al2O3 and theta-Al2O3 phase at 800 degrees C. The SEM appearance of the fibers showed that the addition of boron resulted in the formation of crosslinked bright surfaced fibers.en_US
dc.description.sponsorshipSelcuk University, TurkeySelcuk Universityen_US
dc.description.sponsorshipThis work was supported by the grant of M Sc. Program, Selcuk University, Turkey.en_US
dc.identifier.doi10.1007/s12221-011-0303-1en_US
dc.identifier.endpage309en_US
dc.identifier.issn1229-9197en_US
dc.identifier.issn1875-0052en_US
dc.identifier.issue3en_US
dc.identifier.scopusqualityQ2en_US
dc.identifier.startpage303en_US
dc.identifier.urihttps://dx.doi.org/10.1007/s12221-011-0303-1
dc.identifier.urihttps://hdl.handle.net/20.500.12395/26860
dc.identifier.volume12en_US
dc.identifier.wosWOS:000290739500003en_US
dc.identifier.wosqualityQ2en_US
dc.indekslendigikaynakWeb of Scienceen_US
dc.indekslendigikaynakScopusen_US
dc.language.isoenen_US
dc.publisherKOREAN FIBER SOCen_US
dc.relation.ispartofFIBERS AND POLYMERSen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.selcuk20240510_oaigen_US
dc.subjectElectrospinningen_US
dc.subjectBoric aciden_US
dc.subjectNanofibersen_US
dc.subjectZr-Al acetateen_US
dc.subjectPVAen_US
dc.titleSynthesis and Characterization of Boron Doped Alumina Stabilized Zirconia Fibersen_US
dc.typeArticleen_US

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