Preparation of a New 1,3-Alternate-Calix[4]arene-Bonded HPLC Stationary Phase for the Separation of Phenols, Aromatic Amines and Drugs

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dc.contributor.authorErdemir, Serkan
dc.contributor.authorYılmaz, Mustafa
dc.date.accessioned2020-03-26T18:04:50Z
dc.date.available2020-03-26T18:04:50Z
dc.date.issued2010
dc.departmentSelçuk Üniversitesien_US
dc.description.abstractWe have synthesized the 1,3-alternate 25,27-dioctyloxy-26,28-bis-[3-aminopropyloxy]-calix[4]arene and then immobilized onto gamma-chloropropylsilica gel (CPS). The high-performance liquid chromatographic behavior of some aromatic hydrocarbons, phenolic compounds, aromatic amines and drug compounds was studied on this 1,3-alternate-calix[4]arene-bonded silica gel stationary phase (CIMS). The effect of organic modifier content and pH of the mobile phase on retention and selectivity of these compounds were investigated. According to chromatographic data, it can be concluded that the selectivity of CIMS for analytes ascribes to various interactions between CIMS and the analytes. such as hydrophobic interaction, hydrogen bonding interaction, pi-pi interaction and inclusion interaction.en_US
dc.description.sponsorshipScientific Research Projects Foundation of Selcuk University (SUBAP)Selcuk University [2009-09401040]en_US
dc.description.sponsorshipWe thank the Scientific Research Projects Foundation of Selcuk University (SUBAP-Grant Number 2009-09401040) for financial support of this work produced from a part of S. Erdemir's PhD Thesis.en_US
dc.identifier.citationErdemir, S., Yılmaz, M., (2010). Preparation of a New 1,3-Alternate-Calix[4]arene-Bonded HPLC Stationary Phase for the Separation of Phenols, Aromatic Amines and Drugs. Talanta, (82), 1240-1246. Doi: 10.1016/j.talanta.2010.06.063
dc.identifier.doi10.1016/j.talanta.2010.06.063en_US
dc.identifier.endpage1246en_US
dc.identifier.issn0039-9140en_US
dc.identifier.issn1873-3573en_US
dc.identifier.pmid20801324en_US
dc.identifier.scopusqualityQ1en_US
dc.identifier.startpage1240en_US
dc.identifier.urihttps://dx.doi.org/10.1016/j.talanta.2010.06.063
dc.identifier.urihttps://hdl.handle.net/20.500.12395/25176
dc.identifier.volume82en_US
dc.identifier.wosWOS:000282480500023en_US
dc.identifier.wosqualityQ1en_US
dc.indekslendigikaynakWeb of Scienceen_US
dc.indekslendigikaynakScopusen_US
dc.indekslendigikaynakPubMeden_US
dc.institutionauthorErdemir, Serkan
dc.institutionauthorYılmaz, Mustafa
dc.language.isoenen_US
dc.publisherElsevieren_US
dc.relation.ispartofTalantaen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/openAccessen_US
dc.selcuk20240510_oaigen_US
dc.subjectCalix[4]areneen_US
dc.subjectSilica gelen_US
dc.subjectAromatic aminesen_US
dc.subjectSeparationen_US
dc.subjectHigh-performance liquid chromatographyen_US
dc.titlePreparation of a New 1,3-Alternate-Calix[4]arene-Bonded HPLC Stationary Phase for the Separation of Phenols, Aromatic Amines and Drugsen_US
dc.typeArticleen_US

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