Determination of Selected Polychlorinated Biphenyls in Soil by Miniaturised Ultrasonic Solvent Extraction and Gas Chromatography-Mass-Selective Detection

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dc.contributor.authorAydın, Mehmet Emin
dc.contributor.authorTor, Ali
dc.contributor.authorÖzcan, Senar
dc.date.accessioned2020-03-26T17:03:21Z
dc.date.available2020-03-26T17:03:21Z
dc.date.issued2006
dc.departmentSelçuk Üniversitesien_US
dc.description.abstractMiniaturised ultrasonic solvent extraction procedure was developed for the determination of selected polychlorinated biphenyls (PCBs) in soil samples by gas chromatography-mass-selective detection by using 2(3) factorial experimental design. Recoveries of PCBs from fortified soil samples are over 90% for three different fortification levels between 40 and 120 mu g kg(-1), and relative standard deviations of the recoveries are below 7%. The limits of detection (LODs) ranged from 0.003 to 0.006 mu g kg(-1). The performance of the proposed method was compared to traditional shake flask extraction method on the spiked real soil sample and extraction methods showed comparable efficiencies. Proposed miniaturised ultrasonic solvent extraction offers several advantages, i.e., reducing sample requirement for measurement of target compound, less solvent consumption and reducing the costs associated with solvent purchase and waste disposal.en_US
dc.identifier.citationAydın, M. E., Tor, A., Özcan, S., (2006). Determination of Selected Polychlorinated Biphenyls in Soil by Miniaturised Ultrasonic Solvent Extraction and Gas Chromatography-Mass-Selective Detection. Analytica Chimica Acta, (577), 232-237. Doi: 10.1016/j.aca.2006.06.050
dc.identifier.doi10.1016/j.aca.2006.06.050en_US
dc.identifier.endpage237en_US
dc.identifier.issn0003-2670en_US
dc.identifier.pmid17723677en_US
dc.identifier.scopusqualityQ1en_US
dc.identifier.startpage232en_US
dc.identifier.urihttps://dx.doi.org/10.1016/j.aca.2006.06.050
dc.identifier.urihttps://hdl.handle.net/20.500.12395/20430
dc.identifier.volume577en_US
dc.identifier.wosWOS:000240569500012en_US
dc.identifier.wosqualityQ1en_US
dc.indekslendigikaynakWeb of Scienceen_US
dc.indekslendigikaynakScopusen_US
dc.indekslendigikaynakPubMeden_US
dc.institutionauthorAydın, Mehmet Emin
dc.institutionauthorTor, Ali
dc.institutionauthorÖzcan, Senar
dc.language.isoenen_US
dc.publisherElsevier Science Bven_US
dc.relation.ispartofAnalytica Chimica Actaen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/openAccessen_US
dc.selcuk20240510_oaigen_US
dc.subjectmicro-scale extractionen_US
dc.subjectultrasonic solvent extractionen_US
dc.subjectpolychlorinated biphenylsen_US
dc.subjectsoilen_US
dc.subjectfactorial designen_US
dc.titleDetermination of Selected Polychlorinated Biphenyls in Soil by Miniaturised Ultrasonic Solvent Extraction and Gas Chromatography-Mass-Selective Detectionen_US
dc.typeArticleen_US

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